Spectrum Details
NP-MRD ID:NP0289651
Compound name:(1's,2r,2's,4's,5r,7's,8'r,9's,12's,13'r,15'r,16'r)-5,7',9',13'-tetramethyl-5'-oxaspiro[oxane-2,6'-pentacyclo[10.8.0.0²,⁹.0⁴,⁸.0¹³,¹⁸]icosan]-18'-ene-15',16'-diol
Spectrum type:1H NMR Spectrum (1D, 300 MHz, H2O, predicted)
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?JSV
Multiplets 
5.31
4.38
3.42
3.39
3.31
2.53
1.87
1.79
1.78
1.64
1.64
1.61
1.54
1.54
1.49
1.45
1.10
1.02
1.00
0.98
0.87
0.78
Peak Assignment Table
Row No.Cluster MidpointNo. PeaksCoupling TypeNo. H'sAtom No.Peak Centers (ppm)
15.318dd1
44
5.265.265.305.315.315.325.365.36
24.3810ddd1
37
4.324.324.344.374.374.394.394.424.444.44
33.428dd2
72
73
3.383.423.423.463.393.423.423.45
43.3933ddd2
47
49
3.343.353.363.363.373.383.383.393.403.403.403.413.413.423.423.433.333.353.353.363.373.383.383.393.393.403.403.403.413.413.423.433.43
53.3121dd2
51
52
3.213.293.293.293.313.323.333.343.353.363.243.253.273.283.303.313.313.323.333.353.36
62.539dd2
45
46
2.512.512.532.542.502.512.532.532.58
71.878m1
35
1.831.841.851.861.881.891.901.91
81.7915ddd2
42
43
1.751.761.771.781.801.811.831.721.731.771.781.801.811.851.86
91.784dd1
36
1.761.771.791.80
101.6415ddd2
38
39
1.571.601.611.641.641.671.681.711.601.611.631.641.651.671.68
111.6436ddd2
64
65
1.551.561.571.581.581.591.611.611.621.621.631.631.641.661.671.681.691.701.701.701.721.731.551.581.591.601.601.611.621.631.641.651.661.661.681.71
121.6139m1
68
1.521.531.541.541.551.551.561.561.561.571.571.571.581.581.581.591.591.601.601.601.611.621.621.621.621.631.631.641.651.651.661.661.671.671.671.681.691.691.71
131.5449m2
66
67
1.421.481.501.501.511.511.521.521.521.531.541.541.541.551.551.561.571.591.611.451.451.461.471.471.491.491.491.501.511.511.521.521.531.541.541.541.551.561.561.571.581.581.591.601.601.611.621.641.65
141.5432m1
41
1.451.461.471.491.491.491.501.501.501.501.511.511.521.531.541.541.541.541.541.551.551.561.571.571.571.581.581.581.591.591.611.63
151.4940m2
57
58
1.391.411.431.441.451.461.471.481.481.491.501.521.521.521.531.541.551.561.561.591.431.441.441.451.461.471.471.481.481.491.491.501.501.521.521.531.541.541.561.56
161.4539ddd2
59
60
1.371.391.391.391.401.421.421.431.441.441.451.451.461.461.471.481.491.501.501.511.521.541.361.391.411.431.431.431.441.451.451.461.461.471.471.471.481.501.50
171.1015ddd1
40
1.041.051.071.081.081.081.091.111.111.121.121.121.131.151.16
181.021s3
53
54
55
1.02
191.0049ddd1
56
0.880.900.910.910.920.920.930.930.930.940.940.950.950.960.960.960.970.970.980.980.990.990.991.001.001.001.001.011.011.021.021.031.031.041.041.051.051.051.061.061.071.071.081.081.091.091.101.111.13
200.983t3
32
33
34
0.970.970.99
210.873t3
69
70
71
0.860.860.88
220.781s3
61
62
63
0.78
Experimental Conditions
Solvent:H2O
Nucleus:1H
Frequency:300 MHz
Documentation
Document DescriptionDownloadFile Size
Peak List (TXT)Download file24 KB
Peak Assignments (TXT)Download file1.29 KB
Spectra Image with Peak AssignmentsNot AvailableNot Available
Raw Spectrum ImageNot AvailableNot Available
nmrML File (NMRML)Download file596 KB
JCAMP-DX File (JDX)Download file186 KB
Raw Free Induction Decay file for spectral processingNot AvailableNot Available
Validation ReportNot AvailableNot Available
References
Not Available