Spectrum Details
NP-MRD ID:NP0287349
Compound name:(6r)-6-[(1r,3as,3bs,7s,9as,9bs,11ar)-9a-(hydroxymethyl)-11a-methyl-7-{[(2s,3s,4r,5r)-3,4,5-trihydroxyoxan-2-yl]oxy}-1h,2h,3h,3ah,3bh,4h,6h,7h,8h,9h,9bh,10h,11h-cyclopenta[a]phenanthren-1-yl]-2-methylheptan-2-yl acetate
Spectrum type:1H NMR Spectrum (1D, 400 MHz, H2O, predicted)
Spectrum View
Spectra Viewer Instructions...

Spectra Viewer Controls

ActionCommand
Zoom In/Out X AxisScroll wheel
Zoom In/Out Y AxisAlt/Option Key + Scroll wheel
Zoom In on AreaAlt/Option Key + Click and Drag around area
Zoom Out CompletelyAlt/Option Key + Click once anywhere on viewer
Move AroundClick and Drag

Zoombox Controls (box in upper left corner)

ActionCommand
Move AroundClick and Drag grey selection box
Zoom In on AreaClick on unselected region and drag around new selection
Zoom Out CompletelyClick once anywhere in unselected region
Alter Zoomed AreaClick and Drag on sides of grey selection box

Troubleshooting

If the viewer is not showing any spectra or is slow, try updating to the latest version of your browser. We have found that Google Chrome is the fastest.



?JSV
Multiplets 
5.34
4.80
4.40
4.14
4.09
4.04
4.01
3.74
2.39
2.02
1.97
1.94
1.73
1.72
1.64
1.61
1.56
1.50
1.43
1.36
1.32
1.31
1.27
1.16
1.15
0.95
0.94
0.64
Peak Assignment Table
Row No.Cluster MidpointNo. PeaksCoupling TypeNo. H'sAtom No.Peak Centers (ppm)
15.348dd1
71
5.305.305.335.345.345.355.385.38
24.804q1
75
4.774.804.804.83
34.401s2
88
89
4.40
44.148dd2
76
77
4.114.144.154.174.124.144.144.16
54.099ddd1
78
4.064.074.084.094.094.104.114.124.13
64.044dd1
80
4.034.044.044.05
74.013dd1
82
4.004.014.02
83.7423m1
74
3.683.693.693.693.703.703.713.723.723.733.743.743.753.763.763.773.783.783.793.793.793.793.80
92.398dd2
72
73
2.342.382.402.442.362.382.402.42
102.0244ddd2
69
70
1.941.951.971.971.981.981.981.992.002.002.012.012.012.032.032.032.032.042.042.052.062.072.072.082.082.082.092.101.961.961.971.971.991.992.002.002.002.012.012.032.042.042.052.07
111.971s3
43
44
45
1.97
121.9431m2
84
85
1.891.901.921.931.931.931.931.951.951.951.971.982.001.871.901.901.911.911.921.931.941.941.941.941.951.961.971.981.981.982.01
131.7331ddd2
94
95
1.671.691.691.711.711.721.731.751.751.761.771.801.671.681.681.691.701.711.721.721.731.731.731.741.751.771.771.771.781.791.82
141.7230ddd2
86
87
1.661.671.681.691.701.711.721.721.721.731.741.751.751.761.771.781.651.681.681.691.701.711.721.721.721.731.741.751.761.78
151.6446m2
63
64
1.571.591.591.591.611.621.621.621.631.631.631.641.641.651.651.651.661.661.671.681.691.691.691.721.561.581.591.601.601.611.621.631.631.631.641.641.651.651.651.661.671.681.691.691.701.72
161.6123ddd1
91
1.541.541.561.561.561.571.571.581.591.601.601.611.611.611.611.621.631.641.651.661.661.681.68
171.5639m1
68
1.481.481.501.501.511.511.521.531.531.531.531.541.541.541.541.551.551.551.561.561.561.571.571.571.581.581.581.581.591.591.601.601.601.611.611.621.621.631.63
181.5057m2
92
93
1.421.421.431.431.441.451.451.451.461.471.481.481.491.491.501.501.501.501.501.511.511.521.531.531.541.541.541.551.551.561.571.571.411.441.451.461.471.471.481.481.481.491.491.501.501.511.511.521.521.521.521.531.541.541.551.551.55
191.4317t2
52
53
1.401.411.461.381.411.421.421.421.431.431.431.441.451.451.451.451.47
201.3632tt2
54
55
1.311.321.351.351.361.371.371.371.371.381.381.401.291.321.341.341.351.351.351.361.361.361.361.371.371.371.381.381.391.391.401.44
211.3232m2
65
66
1.271.281.291.301.311.311.311.321.321.321.331.331.341.351.371.371.251.261.281.291.291.311.311.321.321.321.331.331.351.361.381.40
221.311s6
46
47
48
49
50
51
1.31
231.2729td2
56
57
1.231.301.301.311.321.341.181.191.201.221.221.221.231.231.231.241.251.251.261.271.281.281.301.311.311.311.321.331.34
241.1625ddd1
67
1.091.101.111.111.121.121.131.141.141.151.151.151.151.161.171.171.171.181.191.201.201.201.211.211.23
251.1522m1
58
1.081.101.101.101.111.121.121.131.131.131.141.141.151.151.151.161.161.171.181.231.241.25
260.956ddd1
62
0.920.930.940.960.970.98
270.945quint3
59
60
61
0.930.950.930.930.95
280.641s3
96
97
98
0.64
Experimental Conditions
Solvent:H2O
Nucleus:1H
Frequency:400 MHz
Documentation
Document DescriptionDownloadFile Size
Peak List (TXT)Download file31.5 KB
Peak Assignments (TXT)Download file1.62 KB
Spectra Image with Peak AssignmentsNot AvailableNot Available
Raw Spectrum ImageNot AvailableNot Available
nmrML File (NMRML)Download file608 KB
JCAMP-DX File (JDX)Download file196 KB
Raw Free Induction Decay file for spectral processingNot AvailableNot Available
Validation ReportNot AvailableNot Available
References
Not Available