Spectrum Details
NP-MRD ID:NP0271738
Compound name:(1s,3as,3bs,7r,9s,9ar,9bs,11as)-1-[(2r,3r)-2,3-dihydroxy-4-[(3s,4r)-4-methyl-5-oxooxolan-3-yl]butan-2-yl]-7-hydroxy-9a,11a-dimethyl-1h,2h,3h,3ah,3bh,4h,6h,7h,8h,9h,9bh,10h,11h-cyclopenta[a]phenanthren-9-yl acetate
Spectrum type:1H NMR Spectrum (1D, 300 MHz, H2O, predicted)
Spectrum View
Spectra Viewer Instructions...

Spectra Viewer Controls

ActionCommand
Zoom In/Out X AxisScroll wheel
Zoom In/Out Y AxisAlt/Option Key + Scroll wheel
Zoom In on AreaAlt/Option Key + Click and Drag around area
Zoom Out CompletelyAlt/Option Key + Click once anywhere on viewer
Move AroundClick and Drag

Zoombox Controls (box in upper left corner)

ActionCommand
Move AroundClick and Drag grey selection box
Zoom In on AreaClick on unselected region and drag around new selection
Zoom Out CompletelyClick once anywhere in unselected region
Alter Zoomed AreaClick and Drag on sides of grey selection box

Troubleshooting

If the viewer is not showing any spectra or is slow, try updating to the latest version of your browser. We have found that Google Chrome is the fastest.



?JSV
Multiplets 
5.34
4.77
4.08
4.04
3.93
2.63
2.44
2.30
2.29
2.12
2.01
2.01
1.88
1.59
1.58
1.58
1.56
1.54
1.48
1.47
1.47
1.25
1.25
1.18
1.17
0.94
Peak Assignment Table
Row No.Cluster MidpointNo. PeaksCoupling TypeNo. H'sAtom No.Peak Centers (ppm)
15.348dd1
48
5.295.295.335.345.345.355.395.39
24.775dd1
41
4.734.754.774.794.81
34.083t1
62
4.064.084.10
44.044dd2
67
68
4.024.064.024.06
53.9315m1
44
3.873.883.893.903.913.923.923.933.943.943.953.963.973.983.99
62.638m1
69
2.592.602.612.632.632.652.662.67
72.448dd2
46
47
2.402.432.452.482.382.432.452.50
82.3018m1
66
2.242.262.262.272.282.282.292.292.302.302.312.312.322.322.332.342.342.36
92.2927dd1
57
2.152.172.192.212.242.252.252.262.262.292.292.292.292.302.312.312.322.322.332.332.342.352.352.372.392.392.42
102.1216ddd2
42
43
2.062.072.102.112.132.142.172.182.082.092.112.122.122.132.152.16
112.0143ddd2
49
50
1.921.941.951.961.961.971.981.992.002.012.022.032.032.032.042.042.052.072.082.082.092.092.102.111.921.941.951.961.971.971.971.981.991.992.002.002.012.012.032.042.042.052.07
122.011s3
38
39
40
2.01
131.883dd2
64
65
1.861.881.90
141.5940ddd1
80
1.521.521.531.531.531.541.541.551.551.551.551.561.561.561.571.571.581.581.591.591.601.601.601.601.611.611.611.611.631.631.631.641.641.641.651.661.671.681.681.69
151.5824m1
56
1.521.521.531.531.541.551.551.561.561.571.571.581.581.591.591.601.601.601.611.641.641.641.661.67
161.5830m1
55
1.491.491.511.511.511.521.531.531.531.541.551.561.561.571.571.581.591.591.601.601.601.621.631.631.641.641.651.661.671.67
171.5643m1
51
1.451.451.461.471.471.471.481.491.501.511.511.521.531.531.541.541.541.541.551.551.551.561.561.561.561.571.571.581.581.591.591.601.601.611.611.621.631.641.641.641.651.651.65
181.542s3
58
59
60
1.541.54
191.4833m1
54
1.371.391.401.411.421.421.421.431.431.441.451.461.461.461.471.471.481.481.491.491.491.501.501.511.521.531.531.541.541.551.551.551.57
201.4725m1
53
1.391.401.421.421.431.441.451.461.461.471.471.481.481.491.491.491.501.501.501.511.511.521.521.531.55
211.4762m2
78
79
1.371.401.401.411.411.421.421.441.451.451.461.461.461.461.471.481.481.491.491.491.491.501.501.521.531.531.551.371.371.391.391.391.411.411.421.421.431.431.451.451.451.461.461.471.471.481.481.481.481.491.491.511.511.521.521.531.531.541.551.551.561.57
221.253t3
70
71
72
1.261.241.26
231.251s3
81
82
83
1.25
241.1832ddd2
76
77
1.081.101.101.121.131.141.161.171.171.181.191.211.221.231.251.281.301.091.121.121.151.161.161.171.171.181.191.201.211.211.221.26
251.1747ddd1
52
1.051.061.061.071.081.091.091.091.101.101.111.111.121.121.131.131.141.141.141.141.151.151.161.171.171.171.181.181.191.191.201.201.221.221.231.231.241.241.251.251.261.261.271.291.291.301.31
260.941s3
73
74
75
0.94
Experimental Conditions
Solvent:H2O
Nucleus:1H
Frequency:300 MHz
Documentation
Document DescriptionDownloadFile Size
Peak List (TXT)Download file27.5 KB
Peak Assignments (TXT)Download file1.37 KB
Spectra Image with Peak AssignmentsNot AvailableNot Available
Raw Spectrum ImageNot AvailableNot Available
nmrML File (NMRML)Download file603 KB
JCAMP-DX File (JDX)Download file192 KB
Raw Free Induction Decay file for spectral processingNot AvailableNot Available
Validation ReportNot AvailableNot Available
References
Not Available