1H NMR Spectrum (1D, 100 MHz, D2O, predicted) (NP0007924)
Spectrum Details
| NP-MRD ID: | NP0007924 |
|---|---|
| Compound name: | 12b-acetoxy-3b-hydroxy-7,11,15,23-tetraoxo-lanost-8,20E-diene-26-oic acid |
| Spectrum type: | 1H NMR Spectrum (1D, 100 MHz, D2O, predicted) |
Spectrum View
Spectra Viewer Instructions...
Spectra Viewer Controls
| Action | Command |
|---|---|
| Zoom In/Out X Axis | Scroll wheel |
| Zoom In/Out Y Axis | Alt/Option Key + Scroll wheel |
| Zoom In on Area | Alt/Option Key + Click and Drag around area |
| Zoom Out Completely | Alt/Option Key + Click once anywhere on viewer |
| Move Around | Click and Drag |
Zoombox Controls (box in upper left corner)
| Action | Command |
|---|---|
| Move Around | Click and Drag grey selection box |
| Zoom In on Area | Click on unselected region and drag around new selection |
| Zoom Out Completely | Click once anywhere in unselected region |
| Alter Zoomed Area | Click and Drag on sides of grey selection box |
Troubleshooting
If the viewer is not showing any spectra or is slow, try updating to the latest version of your browser. We have found that Google Chrome is the fastest.
| Peak Assignment Table | |||||||
|---|---|---|---|---|---|---|---|
| Row No. | Cluster Midpoint | No. Peaks | Coupling Type | No. H's | Atom No. | Peak Centers (ppm) | |
| 1 | 6.32 | 4 | dq | 1 | 73 | 6.316.326.326.33 | |
| 2 | 2.86 | 4 | dd | 1 | 55 | 2.832.852.882.89 | |
| 3 | 2.52 | 11 | m | 1 | 76 | 2.362.412.442.472.492.502.552.562.612.622.68 | |
| 4 | 2.43 | 8 | dd | 2 | 67 68 | 2.212.392.482.662.282.382.462.56 | |
| 5 | 2.38 | 8 | dd | 1 | 74 | 2.232.282.292.342.442.442.492.50 | |
| 6 | 2.31 | 5 | dd | 1 | 47 | 2.172.302.312.332.44 | |
| 7 | 2.18 | 9 | dd | 1 | 75 | 2.072.082.092.112.162.232.302.302.31 | |
| 8 | 2.16 | 14 | m | 1 | 58 | 2.012.032.052.082.102.122.142.162.182.192.202.232.252.45 | |
| 9 | 2.13 | 1 | s | 2 | 42 43 | 2.13 | |
| 10 | 2.11 | 12 | ddd | 1 | 69 | 1.911.922.012.032.092.102.112.122.192.202.292.30 | |
| 11 | 2.09 | 4 | dd | 1 | 48 | 2.022.032.152.16 | |
| 12 | 2.02 | 5 | dd | 1 | 46 | 1.851.992.002.132.14 | |
| 13 | 2.01 | 8 | ddd | 1 | 59 | 1.931.941.971.992.042.072.082.11 | |
| 14 | 1.71 | 10 | ddd | 1 | 60 | 1.561.581.601.641.651.711.781.831.881.89 | |
| 15 | 1.62 | 2 | d | 3 | 70 71 72 | 1.621.62 | |
| 16 | 1.59 | 1 | s | 1 | 45 | 1.59 | |
| 17 | 1.40 | 17 | m | 1 | 57 | 1.231.241.271.291.341.351.351.361.381.391.411.451.471.491.511.611.66 | |
| 18 | 1.15 | 1 | s | 1 | 64 | 1.15 | |
| 19 | 1.15 | 1 | s | 2 | 65 66 | 1.15 | |
| 20 | 1.08 | 16 | m | 3 | 77 78 79 | 1.051.101.251.041.100.900.971.011.021.041.051.091.101.121.171.22 | |
| 21 | 1.04 | 3 | t | 1 | 49 | 0.900.991.23 | |
| 22 | 0.97 | 4 | t | 1 | 52 | 0.850.941.001.09 | |
| 23 | 0.97 | 2 | d | 1 | 51 | 0.891.04 | |
| 24 | 0.75 | 3 | t | 1 | 53 | 0.600.750.89 | |
| 25 | 0.71 | 1 | s | 2 | 61 62 | 0.71 | |
| 26 | 0.71 | 1 | s | 2 | 81 82 | 0.71 | |
| 27 | 0.68 | 4 | t | 1 | 50 | 0.560.650.710.80 | |
| 28 | 0.58 | 5 | t | 1 | 54 | 0.400.510.600.650.74 | |
Experimental Conditions
| Solvent: | D2O |
|---|---|
| Nucleus: | 1H |
| Frequency: | 100 MHz |
Documentation
| Document Description | Download | File Size |
|---|---|---|
| Peak List (TXT) | Download file | 9.16 KB |
| Peak Assignments (TXT) | Download file | 1.28 KB |
| Spectra Image with Peak Assignments | Not Available | Not Available |
| Raw Spectrum Image | Not Available | Not Available |
| nmrML File (NMRML) | Download file | 575 KB |
| JCAMP-DX File | Not Available | Not Available |
| Raw Free Induction Decay file for spectral processing | Not Available | Not Available |
| Validation Report | Not Available | Not Available |
References
Not Available