##TITLE=NP0000539, Submission ID 402, Experimental spectrum ##JCAMP-DX=4.24 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATA TYPE=LINK ##DATE=22/01/08 ##TIME=17:08:42 ##LONG DATE=2022/01/08 17:08:42 ##TITLE=1-Methylhistidine ##JCAMP-CS=3.7 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATE=22/01/08 ##TIME=17:08:42 ##BLOCK_ID=1 ##CROSS REFERENCE=NMR PEAK ASSIGNMENTS:BLOCK_ID=4 ##LONG DATE=2022/01/08 17:08:42 ##MOLFORM=C7 H11 N3 O2 ##ATOMLIST= 1 C 0 2 N 0 3 C 0 4 N 0 5 C 0 6 C 0 7 C 0 8 N 0 9 C 0 10 O 0 11 O 0 12 C 0 13 H 0 14 H 0 15 H 0 16 H 0 17 H 0 18 H 0 19 H 0 20 H 0 21 H 0 22 H 0 23 H 0 ##BONDLIST= 1 2 S 2 3 S 3 4 D 4 5 S 5 6 S 6 7 S 7 8 S 7 9 S 9 10 D 9 11 S 5 12 D 12 2 S 1 13 S 1 14 S 1 15 S 3 16 S 6 17 S 6 18 S 7 19 S 8 20 S 8 21 S 11 22 S 12 23 S ##STEREOCENTER= 7 M 0 ##$MOLFILE= RDKit 3D 23 23 0 0 0 0 0 0 0 0999 V2000 -3.7965 0.4448 0.6288 C 0 0 0 0 0 0 0 0 0 0 0 0 -2.5143 0.2030 -0.0219 N 0 0 0 0 0 0 0 0 0 0 0 0 -2.1833 0.5729 -1.2700 C 0 0 0 0 0 0 0 0 0 0 0 0 -0.9076 0.1722 -1.5171 N 0 0 0 0 0 0 0 0 0 0 0 0 -0.4233 -0.4517 -0.4322 C 0 0 0 0 0 0 0 0 0 0 0 0 0.9362 -1.0633 -0.2343 C 0 0 0 0 0 0 0 0 0 0 0 0 1.8694 0.0073 0.3365 C 0 0 2 0 0 0 0 0 0 0 0 0 1.9190 1.0715 -0.6098 N 0 0 0 0 0 0 0 0 0 0 0 0 3.1758 -0.6357 0.5676 C 0 0 0 0 0 0 0 0 0 0 0 0 3.3182 -1.5901 1.3685 O 0 0 0 0 0 0 0 0 0 0 0 0 4.2848 -0.1797 -0.1150 O 0 0 0 0 0 0 0 0 0 0 0 0 -1.4459 -0.4252 0.5022 C 0 0 0 0 0 0 0 0 0 0 0 0 -3.8709 1.5444 0.7697 H 0 0 0 0 0 0 0 0 0 0 0 0 -4.5730 0.0604 -0.0609 H 0 0 0 0 0 0 0 0 0 0 0 0 -3.8362 -0.0965 1.5839 H 0 0 0 0 0 0 0 0 0 0 0 0 -2.8121 1.1001 -1.9720 H 0 0 0 0 0 0 0 0 0 0 0 0 1.3668 -1.3756 -1.1928 H 0 0 0 0 0 0 0 0 0 0 0 0 0.8302 -1.9195 0.4364 H 0 0 0 0 0 0 0 0 0 0 0 0 1.4528 0.3825 1.2929 H 0 0 0 0 0 0 0 0 0 0 0 0 1.9969 0.7949 -1.5912 H 0 0 0 0 0 0 0 0 0 0 0 0 2.4196 1.9129 -0.3210 H 0 0 0 0 0 0 0 0 0 0 0 0 4.1752 0.3217 -0.9697 H 0 0 0 0 0 0 0 0 0 0 0 0 -1.3819 -0.8513 1.5043 H 0 0 0 0 0 0 0 0 0 0 0 0 1 2 1 0 2 3 1 0 3 4 2 0 4 5 1 0 5 6 1 0 6 7 1 0 7 8 1 0 7 9 1 0 9 10 2 0 9 11 1 0 5 12 2 0 12 2 1 0 1 13 1 0 1 14 1 0 1 15 1 0 3 16 1 0 6 17 1 0 6 18 1 0 7 19 1 1 8 20 1 0 8 21 1 0 11 22 1 0 12 23 1 0 M END ##END= ##TITLE=Experimental spectrum ##JCAMP-DX=5.01 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATA TYPE=NMR SPECTRUM ##BLOCK_ID=2 ##DATE=22/01/08 ##TIME=17:08:42 ##TEMPERATURE=NA ##LONG DATE=2022/01/08 17:08:42 ##.OBSERVE FREQUENCY=700.0 ##.OBSERVE NUCLEUS=1H ##.SOLVENT NAME=H2O ##.SHIFT REFERENCE=INTERNAL,DSS,58890.00,0 ##XUNITS=PPM ##FIRSTX=10.800733229966022 ##LASTX=-1.218727667059336 ##MINX=-1.218727667059336 ##MAXX=10.800733229966022 ##XFACTOR=0.00018340521701354362 ##NPOINTS=65536 ##YUNITS=ARBITRARY UNITS ##FIRSTY=-0.13925844032957838 ##LASTY=0.06504900351048275 ##MINY=-6.759660547032627 ##MAXY=10000.0 ##YFACTOR=0.3051850947599719 ##XYDATA=(X++(Y..Y)), XYDATA $$ DIF 58890@j%%%J%%%%%%J%%%jJ%%%J%%%%J%j%%%%%%%%%%%%J%%%%j%j%%jJ%%j%%j%%%%J%%%%%%j%J%% 58816@J%%%%j%%j%%J%%%J%%%%j%%%%%%%%%%%%%%%%%J%%%%%j%%%%%%%jJ%%%%%%%%%%%%%jJ%%%J% 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-6162a%%%%JJ%%%j%%%%j%%%%%%J%%J%%j%%%j%%J%%J%%%j%%%%%%%%%%%jJ%j%%%%J%%%J%%%%j%%% -6236@%%%%%%%%%J%%%j%j%%j%J%J%%%%%%%%%%%j%%%%%%%%%%%%%%%%J%J%%Jj%j%%%%j%j%%J%%%% -6310a%%%%%J%j%%%%j%%%%JJ%%%%j%%%%%J%%%%%%j%j%%%%%%%%%J%%%%%%%%%%%J%J%%%j%%%%%%% -6384@%%%%%%%%%J%%%%%j%%%J%j%j%%j%J%%J%%%%%j%J%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% -6458@%%%%%%%%%%%%%j%%%%%%%J%%%j%%J%%%%%%%J%%%%%%%j%%j%J%%%%%%%%%j%%%j%%J%%j%%%% -6532b%%%%%J%%%%%%%%%%%J%%%%%%%%%%%%j%%J%%%%%%J%%jj%%%%%J%%%%%%J%%%j%%%J%%%%%%%% -6606A%j%%%%%%%%%%%j%%J%%%%%J%%%%j%%%%%j%%%J% -6645@ $$ checkpoint ##END= ##TITLE=Simulated peaks ##JCAMP-DX=5.01 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATA TYPE=NMR PEAK TABLE ##DATA CLASS=PEAK TABLE ##BLOCK_ID=3 ##DATE=22/01/08 ##TIME=17:08:42 ##TEMPERATURE=NA ##LONG DATE=2022/01/08 17:08:42 ##.OBSERVE FREQUENCY=700.0 ##.OBSERVE NUCLEUS=1H ##.SOLVENT NAME=H2O ##NPOINTS=17 ##XUNITS=PPM ##YUNITS=ARBITRARY UNITS ##PEAK TABLE=(XY..XY) (3.6899566650390625, 921.2681953355769) (3.6899566650390625, 921.2681953355769) (3.6899566650390625, 921.2681953355769) (7.6900482177734375, 923.2445366410786) (3.1744842529296875, 233.95982465106925) (3.1676483154296875, 234.3692035663312) (3.152374267578125, 234.14902259986036) (3.145538330078125, 233.21717081309814) (3.086578369140625, 232.39929758717878) (3.0755767822265625, 233.29518596039617) (3.0644683837890625, 232.47539332020546) (3.053466796875, 231.65104236681486) (3.9689483642578125, 234.7309831242491) (3.9621124267578125, 240.32739661175006) (3.95794677734375, 241.11072179164972) (3.95111083984375, 234.18176074951182) (7.009979248046875, 924.3558138956541) ##END= ##TITLE=Assignments ##JCAMP-DX=5.01 ##ORIGIN=NP-MRD ##OWNER=NP-MRD ##DATA TYPE=NMR PEAK ASSIGNMENTS ##DATA CLASS=PEAK ASSIGNMENTS ##BLOCK_ID=4 ##CROSS REFERENCE=STRUCTURE:BLOCK_ID=1 ##DATE=22/01/08 ##TIME=17:08:42 ##TEMPERATURE=NA ##LONG DATE=2022/01/08 17:08:42 ##SOURCE REFERENCE=PMID 31401679 ##.OBSERVE FREQUENCY=700.0 ##.OBSERVE NUCLEUS=1H ##.SOLVENT NAME=H2O ##NPOINTS=17 ##XUNITS=PPM ##PEAK ASSIGNMENTS=(XMA) (3.69, , <13>) (3.69, , <14>) (3.69, , <15>) (7.69, , <16>) (3.16,
, <17>) (3.16,
, <17>) (3.16,
, <17>) (3.16,
, <17>) (3.07,
, <18>) (3.07,
, <18>) (3.07,
, <18>) (3.07,
, <18>) (3.96,
, <19>) (3.96,
, <19>) (3.96,
, <19>) (3.96,
, <19>) (7.01, , <23>) ##END= ##END=